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Conferences

SANS-Workshop 21./22. Juni
June 21 - June 22

Seminars

Expansion of Research Facilities at the NIST Center for Neutron Research
May 21 14:45 - 15:45

The NIST Center for Neutron Research (NCNR) has just returned to full-time operation after...
Commissioning of the CASCADE detector at MIRA
June 04 14:45 - 15:45

Structural and dynamic study of several magnetic systems by means of Neutron Resonant Spin Echo techniques
June 11 14:45 - 15:45

“ZETA” is a Neutron Resonant Spin Echo (NRSE) option which is currently installed on the thermal...
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Materials Science and Catalysis

Materials design:

For the development of new materials not only the chemical composition is decisive for the technical properties, moreover the distinct phases of the material have to be analyzed, if present. The quantitative phase analysis by means of neutron scattering yields information on sample volumes relevant to real application conditions. In contrast to x-ray or synchrotron radiation volumes in the order of several cm3 can be investigated. In addition, the high penetration depth of neutrons facilitates the use of sophisticated sample environments like cryostats furnaces, pressure cells or pulling machines.

The investigations using neutron beams enables the analysis of morphology, i. e. to determine the shape and size of particles (in the range of 1 nm to 400 nm). Furthermore the distribution of particle sizes can be determined if they, for example, are embedded in a matrix. These measurement categories yield important parameters for the improvement or new development of materials.

The instruments used determine atomic distances of the sample to be investigated by means of a diffraction experiment. The detailed analysis of the diffraction patterns yields information about the atomic structure and quantitative fraction of the phases present.

Catalysis research:

In catalysis research the areas heterogeneous and homogeneous catalysis are distinguished.

In the case of heterogeneous catalysis the catalytic converter and the reactant obey different phases as for example in gas reactions or reactions in solutions accelerated by solid catalysts. This group covers metals (platinum, rhodium, palladium and iron), solid metal oxides (e.g. V2O5) metal salts, zeolites as well as enzymes bound to compartments.

In the case of homogenous catalysis the catalyst and the reactant are in the same phase like the educts of the catalytic reaction. In this case one has the advantage that each molecule is catalytic active and not only the surface like in the heterogeneous catalysis. The homogeneous catalysts comprises acids, bases, metal salt solutions as well as complex enzymes.

By means of neutron scattering the electron density distributions can be determined precisely, which are decisive for the catalytic effect. On the other hand in-situ measurements on the interactions between catalyst and reactant can be performed by means of structure and phase analysis of the catalyst.

 

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Thin film technology:

The area of thin film technology comprises the preparation and investigation of thin layers. This means thin coverages of different substances which overcast material of different matter to improve its properties. The applications range from finishing (e.g. corrosion resistance, surface hardening, optical properties) up to the production of active components in microelectronics or data storage with highest density.

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